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Beilstein J. Org. Chem. 2012, 8, 712–725, doi:10.3762/bjoc.8.80
Graphical Abstract
Scheme 1: Reaction scheme of terminal galactose in poly-LacNAc-glycans (1a–d) or GalNAc in LacDiNAc (2) by ga...
Figure 1: Conversion of 3b (squares) to the corresponding α,β-unsaturated aldehyde 7b (triangles) and side pr...
Scheme 2: Enzymatic modifications of oxidised poly-LacNAc oligomers. A: Elongation of LacNAc-6-aldehyde 3a by...
Scheme 3: A: Labelling of poly-LacNAc oligomers 3a–c and 9a with biotin hydrazide derivative BACH (12) yieldi...
Figure 2: HPLC analysis for the conversion of modified LacNAc oligomers 3a, 15a, and 7a with β3-GlcNAc-transf...
Scheme 4: Chemical conjugation of oxidised poly-LacNAc oligomers with heptasaccharide–linker–NH2 (17) by redu...